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In lithium ion arrays, thermal runaway may propagate from a failing cell to neighboring cells and grow into a large-scale fire in a phenomenon referred to as cascading failure. A new experimental setup was developed to investigate cascading failure using 12 cell arrays constructed from cells of 18650 form factor. Thermal runaway was initiated in one cell using an electric heater and observed to propagate through the array using temperature sensors. Cascading failure was studied in nitrogen or air environment to elucidate the impact of combustion. The cell temperature allowed calculation of row-to-row propagation speed in arrays of different cathode chemistries. The yields of oxygen, carbon monoxide, carbon dioxide, total hydrocarbons and hydrogen were measured; corresponding fire hazards were assessed.
This webinar will focus on the following key topics:
• Thermal runaway propagation
• Thermal runaway hazards
• Failure dynamics
• Flammability and toxicity
• Failure Mitigation and suppression
Presenter
Ahmed Said – Postdoc Fellow, Worcester Polytechnic Institute
Ahmed Said is a Postdoctoral Fellow at the Department of Fire Protection Engineering at Worcester Polytechnic Institute (WPI). He is broadly interested in problems related to fire, combustion, and thermal sciences. He is currently engaged in several projects: fire safety of lithium ion batteries, wildland fires, and fire spread on façade systems. He earned his PhD in Mechanical Engineering in 2020 from the University of Maryland, College Park. He also received his BS and MSc in Mechanical Engineering from Cairo University.
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Electrochemical Impedance Spectroscopy and Its Application to Battery Analysis
Electrochemical Impedance Spectroscopy (EIS) is a well-established experimental technique that has applications in coatings, corrosion, sensors, electrochemical double layer capacitors, batteries among others. The power of EIS partly comes from its ability to access a very wide range of frequencies (typically from MHz to μHz). For batteries, parameters such as the internal resistance, electrode surface capacitance and leakage are accessible at different frequencies across the spectrum. This allows EIS to gather all the relevant information with a single measurement. In this webinar, we will briefly introduce EIS and cover its application to batteries. We will talk about how to analyze typical data and how to gather the relevant information. We will further talk about available instrumentation and their limitations.
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• What is impedance spectroscopy?
• What can impedance spectroscopy do for Battery analysis?
• How can capacitance, internal resistance and leakage be determined using EIS?
• What are the instrumental requirements and limits?Presenter
Chris Beasley – Gamry Instruments
Chris Beasley received a BS in Chemistry from Kutztown University in 2000 and got a PhD in electrochemistry from University of North Carolina at Chapel Hill in 2010. His doctoral dissertation was on using redox-active nanoparticles as supercapacitors. Chris joined Gamry Instruments in 2010.
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Determination of Battery Safety and Performance Parameters Using Adiabatic and Isothermal Calorimetry
FREE Webinar – Thermal Hazard Technology is a proud sponsor of this event.
This presentation describes two main types of calorimetry which can be used to carry out safety and performance testing on batteries. Isothermal calorimeters allow for direct heat measurement on cells during use, while adiabatic calorimeters can measure heat released from batteries during thermal runaway.
Calorimetry can serve as a quantitative scientific method for evaluation of battery safety but it requires appropriate instrumentation. The principles of operation of both types of calorimeters are described along with specific applications within the field of battery testing.
A combination of both technics allows for detailed thermal characterization of lithium-ion and other rechargeable cells, and differences due to chemistry, cell design, cell age, state of charge and cell size can be evaluated.
This webinar will focus on the following key topics:
• The principles of adiabatic and isothermal calorimetry
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• Parameters established by adiabatic safety testing
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• Pressure measurement and gas collectionPresenter
Danny Montgomery – Technical Performance Manager at Thermal Hazard TechnologyDanny Montgomery has worked at Thermal Hazard Technology for 9 years. His current role is Technical Performance Manager; overseeing the lab and technical aspects of instrumentation manufactured by THT. He joined the company in 2009 after graduating from Southampton University with a master’s degree in physics.
Danny’s focus is primarily on lithium battery calorimetry; both adiabatic and isothermal. He oversees the use of calorimeters for customer sample testing as well as installing calorimeter systems and provided training for battery and automotive companies worldwide, such as Panasonic, BMW and Samsung. Danny works in Thermal Hazard Technology’s UK office in Milton Keynes.
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Energy Storage RTE Tutorial Course 3/3: Total Battery System RTE – Ranking and Comparison of Different Battery Chemistries
RTE impacts of HVAC/Ventilation and Inverters will be described. Batteries generate heat, and this must be dissipated by system cooling and/or taken out of the system. Heat generated can be calculated by looking at IR heating and that generated (net) by exothermic reactions. Examples will include LFP, Li-NMC, Lead Acid and Nickel batteries, both when they are fresh, as well as at their end of useful life. The overall ancillary equipment energy usage will be listed for these systems, and a % RTE loss will be calculated for both nominal rate and high rate applications. Commentary will be provided for other systems. RTE will be summarized and ranked for most energy storage battery chemistries including ZA, NaS, LiS, Saltwater, Liquid Metal, Zinc Bromine and Fuel Cells.
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• RTE impacts of Inverters and HVAC
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Dr. Halle Cheeseman – Founder/President at Energy Blues LLCDr. Halle Cheeseman earned a PhD in Electrochemistry & Corrosion from the University of Nottingham in UK, graduating in 1985. She has held several executive positions in the battery industry over the past 32 years, including Sr. VP of R&D at Spectrum Brands and VP of R&D at Exide Technologies. Her specific battery experience includes Lithium Ion, Zinc Air, Nickel Metal Hydride, Nickel Iron, Alkaline and Lead Acid, focusing on Consumer, Industrial, Automotive & Renewable Energy applications. In July 2017, Dr. Cheeseman founded Energy Blues LLC, an energy storage consulting cooperative comprising 20+ subject matter experts.
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Advancing Mining Processes to Make Better Materials for Use in Lithium Ion Batteries
American Manganese Inc has developed a low-cost, environmentally friendly hydrometallurgical process to recover manganese (Mn) from lower grade resources. American Manganese has applied for a patent for their hydrometallurgical process that produces electrolytic manganese metal with low energy and water consumption. American Manganese commissioned R&D contractor, Kemetco Research Inc to determine uses of Artillery Peak manganese resource material to generate high value alternative products. Chemical manganese dioxide (CMD) and lithiated manganese oxide (LixMn2O4) for use in rechargeable batteries were the areas researched.
The research was successful in producing CMD from Artillery Peak resource material with low cation impurities and avoiding processing steps that are known to introduce metallic impurities in the final product. Cation impurities cause capacity fade, whereas metallic impurities are known to cause catastrophic failures (such as fire and explosions) in lithium ion batteries. Working rechargeable lithium ion coin cell battery prototypes were produced from the CMD material.
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• Catastrophic failure of Li Ion batteries caused by metallic impurities that may be introduced from the mining of raw materials
• Conventional mining process to recover MnO2 used to make LiMn2O4
• Research on a new mining process that avoids steps known to introduce metallic impurities to recover MnO2 used to make LiMn2O4Presenter
Norman Chow – President – Kemetco Research, Inc.Norman earned a B.A.Sc. and M.A.Sc. in Metals and Materials Engineering from University of British Columbia. He is a Registered Professional Engineer (P. Eng.) in British Columbia. He has over 15 years of technology development and contract research experience. He is the President of Kemetco Research Inc., which he formed after acquiring the Industrial Process Division of BC Research Inc. BC Research had been in operation for over 60 years as an R&D contractor.
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