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Beyond Electrochemical Analysis – 2D to 4D Correlation of Microstructure and Chemistry in Li-ion Batteries
Single imaging instruments as well as correlative microscopy workflows have demonstrated some unique abilities to support LIB research beyond electrochemical analysis methods. Light microscopy delivers insights about ablation effects & phase orientations in the active material, while scanning electron microscopy (SEM) reveals information about aging effects, nanometer cracks & the composition of the active material. Combining SEM with in-situ Raman spectroscopy extends the traditional SEM capabilities to organic and inorganic material identification. X-ray microscopy, furthermore, delivers 3D non-destructive imaging of full battery packs and localized high-resolution information, thus allowing the identification of regions of interest within the battery material volume. This presentation will demonstrate the application of these techniques to Li-ion battery research, including examples on anode, cathode, binder, and separator materials.
This webinar will focus on the following key topics:
• Introduction to available microscopic investigation techniques
for Li-ion battery research:
– Light Microscopy
– Scanning Electron Microscopy
– X-ray Microscopy
– Raman Spectroscopy
• Review of recent battery imaging studies in published literature
• Case studies on using correlative microscopy to characterize battery performance & failure mechanisms
Presenter
Stefanie Freitag – Market Segment Manager at Carl Zeiss
Stefanie is Market Segment Manager in Materials Research at Carl Zeiss Microscopy in Munich. She holds a Diploma in Engineering Physics, gained first work experiences in a nuclear fusion reactor with a pioneering concept in Greifswald, then worked 3 years in the solar industry in Ulm & Hsinchu, Taiwan. In her current position she analyzes and defines new microscopic solutions for specific materials segments including light microscopy, electron microscopy, x-ray microscopy and chemical methods like Raman spectroscopy.
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Energy Storage RTE Tutorial Course 3/3: Total Battery System RTE – Ranking and Comparison of Different Battery Chemistries
RTE impacts of HVAC/Ventilation and Inverters will be described. Batteries generate heat, and this must be dissipated by system cooling and/or taken out of the system. Heat generated can be calculated by looking at IR heating and that generated (net) by exothermic reactions. Examples will include LFP, Li-NMC, Lead Acid and Nickel batteries, both when they are fresh, as well as at their end of useful life. The overall ancillary equipment energy usage will be listed for these systems, and a % RTE loss will be calculated for both nominal rate and high rate applications. Commentary will be provided for other systems. RTE will be summarized and ranked for most energy storage battery chemistries including ZA, NaS, LiS, Saltwater, Liquid Metal, Zinc Bromine and Fuel Cells.
This webinar will focus on the following key topics:
• RTE impacts of Inverters and HVAC
• RTE impacts for ancillary equipment for different systems
• RTE numbers for most battery systems being considered for energy storage
Presenter
Dr. Halle Cheeseman – Founder/President at Energy Blues LLC
Dr. Halle Cheeseman earned a PhD in Electrochemistry & Corrosion from the University of Nottingham in UK, graduating in 1985. She has held several executive positions in the battery industry over the past 32 years, including Sr. VP of R&D at Spectrum Brands and VP of R&D at Exide Technologies. Her specific battery experience includes Lithium Ion, Zinc Air, Nickel Metal Hydride, Nickel Iron, Alkaline and Lead Acid, focusing on Consumer, Industrial, Automotive & Renewable Energy applications. In July 2017, Dr. Cheeseman founded Energy Blues LLC, an energy storage consulting cooperative comprising 20+ subject matter experts.
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Lithium Ion Capacitors – Combining Energy with Power
FREE Webinar – JSR Micro, Inc. is a proud sponsor of this event.
Lithium Ion Capacitors (LIC) are hybrids of electric double-layer capacitors (EDLCs) and lithium ion batteries (LIB). Combining the reversible non-Faradaic cathode from an EDLC and the reversible Faradaic anode from an LIB results in an ultra or super capacitor with significantly increased energy density, improved float performance and low self-discharge rates. Avoiding the lithium metal oxide cathodes from LIB’s improves the inherent safety and eliminates Cobalt content, however still combines aspects of energy & power of both cell types. The Faradaic intercalation/deintercalation reactions at the anode are capable of generating a significant amount of charge, while the non-Faradaic electrostatic storage of the electrical energy formed at the interface of the electrode and the electrolyte, known as an electric double layer, results in fast charge and discharge capabilities for hundreds of thousands, if not millions of cycles.
This webinar will focus on the following key topics:
• What is an LIC? Technology Introduction
• Key Benefits
• Safety
• EDLC vs LIC
• Applications
Presenter
Jeff Myron – Energy Solutions Program Manager at JSR Micro, Inc.
Since 2011 Jeff has been responsible for business development in North America of JSR group’s environmental energy products including, lithium ion capacitors (LIC) and aqueous battery binders. Jeff joined JSR in 2006 as a Technical Sales Specialist for advanced photoresists utilized in IC manufacturing. Immediately prior to JSR, Jeff worked at Molecular Imprints developing the commercial infrastructure for next generation nano imprint lithography templates. Prior to joining Molecular Imprints, he held various engineering, engineering management & product management positions at Motorola, DuPont Photomask & Brewer Science. Jeff earned a bachelor’s degree in chemistry from Illinois State University in 1990 and an MBA from Webster University in 2001.
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Advancing Mining Processes to Make Better Materials for Use in Lithium Ion Batteries
American Manganese Inc has developed a low-cost, environmentally friendly hydrometallurgical process to recover manganese (Mn) from lower grade resources. American Manganese has applied for a patent for their hydrometallurgical process that produces electrolytic manganese metal with low energy and water consumption. American Manganese commissioned R&D contractor, Kemetco Research Inc to determine uses of Artillery Peak manganese resource material to generate high value alternative products. Chemical manganese dioxide (CMD) and lithiated manganese oxide (LixMn2O4) for use in rechargeable batteries were the areas researched.
The research was successful in producing CMD from Artillery Peak resource material with low cation impurities and avoiding processing steps that are known to introduce metallic impurities in the final product. Cation impurities cause capacity fade, whereas metallic impurities are known to cause catastrophic failures (such as fire and explosions) in lithium ion batteries. Working rechargeable lithium ion coin cell battery prototypes were produced from the CMD material.
This webinar will focus on the following key topics:
• Catastrophic failure of Li Ion batteries caused by metallic impurities that may be introduced from the mining of raw materials
• Conventional mining process to recover MnO2 used to make LiMn2O4
• Research on a new mining process that avoids steps known to introduce metallic impurities to recover MnO2 used to make LiMn2O4
Presenter
Norman Chow – President – Kemetco Research, Inc.
Norman earned a B.A.Sc. and M.A.Sc. in Metals and Materials Engineering from University of British Columbia. He is a Registered Professional Engineer (P. Eng.) in British Columbia. He has over 15 years of technology development and contract research experience. He is the President of Kemetco Research Inc., which he formed after acquiring the Industrial Process Division of BC Research Inc. BC Research had been in operation for over 60 years as an R&D contractor.
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